| Description |
1 online resource |
| Contents |
Title Page; Copyright; Table of Contents; List of Contributors; Foreword; Background; The Book; The Chapters; Chapter 1: Flow Photochemistry -- a Green Technology with a Bright Future; 1.1 Introduction to Synthetic Organic Photochemistry; 1.2 Conventional Batch Photochemistry; 1.3 Continuous-Flow Chemistry; 1.4 Selected Examples of Photochemical Reactions under Flow Conditions; 1.5 Summary, Conclusion, and Outlook; Acknowledgments; References; Chapter 2: Continuous Flow Synthesis Using Recyclable Reaction Media; 2.1 Introduction; 2.2 Continuous Flow Reactions Using an Ionic Liquid |
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2.3 Continuous Flow Reactions Using a Fluorous Solvent2.4 Conclusions; References; Chapter 3: Synthesis and Application of H2O2 in Flow Reactors; 3.1 Introduction; 3.2 The Synthesis of Hydrogen Peroxide from Hydrogen and Oxygen in Flow Process with Microtechnology; 3.3 Application of Hydrogen Peroxide in Microreactors; 3.4 Conclusions; Acknowledgments; References; Chapter 4: Scale-Up of Flow Processes in the Pharmaceutical Industry; 4.1 Introduction; 4.2 Stages of Pharmaceutical Development; 4.3 Sustainability of Supply -- The Role of Continuous Processing |
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4.4 Comparison of Batch to Continuous Large-Scale Processing4.5 Scale-Up of a Flow Process; 4.6 Flow Processes in the Manufacture of Pharmaceuticals: Examples of Scale-Up; 4.7 Summary and Outlook on Future Scale-Up; References; Chapter 5: Organic Synthesis in Flow: Toward Higher Levels of Sustainability; 5.1 Introduction; 5.2 Semi-automated Optimization; 5.3 Self-Optimizing Microreactor Systems; 5.4 Sustainability in Microreactor Technology; 5.5 Conclusion; References; Chapter 6: Sustainable Flow Chemistry in Drug Discovery; 6.1 Introduction; 6.2 Laboratory Equipment |
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6.3 Advantages of Improved Sustainability6.4 Sustainable Drug Discovery; 6.5 Conclusions and Outlook; References; Chapter 7: Flow Tools to Define Waste/Time/Energy-Minimized Protocols; 7.1 Introduction; 7.2 Minimization of Solvents and Reuse of Catalytic Systems; 7.3 Time/Cost/Energy Saving Examples Using Flow Approach; 7.4 Conclusions; Acknowledgments; References; Chapter 8: The Application of Flow Chemistry in the Use of Highly Reactive Intermediates and Reagents; 8.1 Introduction; 8.2 Hydrogenation Reactions in Flow; 8.3 Carbonylation in Flow; 8.4 Organometallic Reagents in Flow |
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8.5 Synthesis of Azides and Diazoacetates in Flow8.6 The Use of Flow Reactors to Prepare Unstable Intermediates Using Photochemistry; 8.7 The Use of Flow Reactors to Prepare Unstable Intermediates Using Electrochemistry; 8.8 Fluorination and Trifluoromethylation in Flow; 8.9 Conclusions; Acknowledgments; References; Chapter 9: Nonconventional Techniques in Sustainable Flow Chemistry; 9.1 Introduction; 9.2 Microwave-Assisted Flow Chemistry; 9.3 Inductive Heating in Flow Chemistry; 9.4 Sonochemistry in Flow Chemistry; 9.5 Organic Electrochemistry in Flow Chemistry; 9.6 Conclusions; References |
| Summary |
This ready reference not only presents the hot and emerging topic of modern flow chemistry, it is also unique in illustrating the important connection to sustainable chemistry. Focusing on more sustainable methods and applications, the text extensively covers every important field from reaction time optimization to waste minimization, and from safety improvements to microwave applications. In addition, green metrics are presented as a key aspect of the book, helping readers to evaluate the efficiency of flow technologies and their impact on the overall efficiency of a chemical process. An invaluable handbook for every chemist working in the laboratory, whether in academia or industry |
| Bibliography |
Includes bibliographical references at the end of each chapters and index |
| Notes |
Vendor-supplied metadata |
| Subject |
Flow chemistry.
|
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SCIENCE -- Chemistry -- General.
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Flow chemistry
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| Form |
Electronic book
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| ISBN |
9783527689101 |
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3527689109 |
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