Description |
1 online resource (x, 541 pages) : illustrations |
Contents |
1. Introduction -- 2. Introducing High-Resolution NMR -- 3. Practical Aspects of High-Resolution NMR -- 4. One-Dimensional Techniques -- 5. Introducing Two-Dimensional and Pulsed Field Gradient NMR -- 6. Correlations Through the Chemical Bond I: Homonuclear Shift Correlation -- 7. Correlations Through the Chemical Bond II: Heteronuclear Shift Correlation -- 8. Separating Shifts and Couplings: J-Resolved and Pure Shift Spectroscopy -- 9. Correlations Through Space: The Nuclear Overhauser Effect -- 10. Diffusion NMR Spectroscopy -- 11. Protein -- Ligand Screening by NMR -- 12. Experimental Methods -- 13. Structure Elucidation and Spectrum Assignment |
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1. Introduction -- 2. Présentation de la RMN à haute résolution -- 3. Aspects pratiques de la RMN à haute résolution -- 4. Techniques unidimensionnelles -- 5. Présentation de la RMN à gradient de champ bidimensionnel et pulsé -- 6. Corrélations à travers la liaison chimique I : corrélation de décalage homonucléaire -- 7. Corrélations à travers la liaison chimique II : corrélation de décalage hétéronucléaire -- 8. Décalages et couplages de séparation : spectroscopie résolue en J et à décalage pur -- 9. Corrélations dans l'espace : l'effet Overhauser nucléaire -- 10. Spectroscopie RMN de diffusion -- 11. Protéine -- Criblage de ligands par RMN -- 12. Méthodes expérimentales -- 13. Élucidation de la structure et attribution du spectre |
Summary |
High-Resolution NMR Techniques in Organic Chemistry, Third Edition describes the most important NMR spectroscopy techniques for the structure elucidation of organic molecules and the investigation of their behaviour in solution. Appropriate for advanced undergraduate and graduate students, research chemists and NMR facility managers, this thorough revision covers practical aspects of NMR techniques and instrumentation, data collection, and spectrum interpretation. It describes all major classes of one- and two-dimensional NMR experiments including homonuclear and heteronuclear correlations, the nuclear Overhauser effect, diffusion measurements, and techniques for studying protein-ligand interactions. A trusted authority on this critical expertise, High-Resolution NMR Techniques in Organic Chemistry, Third Edition is an essential resource for every chemist and NMR spectroscopist |
Bibliography |
Includes bibliographical references and index |
Notes |
Print version record |
Subject |
Nuclear magnetic resonance spectroscopy.
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Organic compounds -- Analysis
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Chemistry, Organic.
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Analytical chemistry -- Technique.
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Overhauser effect (Nuclear physics)
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Ligands.
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Proteins -- Analysis.
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High resolution spectroscopy.
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Chemical structure.
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organic chemistry.
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SCIENCE -- Chemistry -- Analytic.
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Proteins -- Analysis
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Overhauser effect (Nuclear physics)
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Ligands
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High resolution spectroscopy
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Chemical structure
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Analytical chemistry -- Technique
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Chemistry, Organic
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Nuclear magnetic resonance spectroscopy
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Organic compounds -- Analysis
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Form |
Electronic book
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ISBN |
9780080999937 |
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008099993X |
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0080999867 |
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9780080999869 |
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